Palladium-Catalyzed C(sp3)—H Oxygenation via Electrochemical Oxidation - Journal of the American Chemical Society (ACS Publications)

Palladium-Catalyzed C(sp3)—H Oxygenation via Electrochemical Oxidation - Journal of the American Chemical Society (ACS Publications)
previously reported oxidants possess significant disadvantages, including poor atom economy, high cost, and the formation of undesired byproducts. To overcome these issues, we report an electrochemical strategy that takes advantage of anodic oxidation of PdII to induce selective C—O reductive elimination with a variety of oxyanion coupling partners.
 

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